Synthesis of the Antibacterial Benzoquinone Primin and its Water-Soluble Analogue, Primin Acid
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Thieme Publishing
Abstract
The biologically active natural product, primin and its water-soluble acid analogue, primin acid are prepared in 34% and 25% overall yields, respectively, from a common intermediate using a Grignard reaction and a Johnson-Claisen rearrangement as the key steps.
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Synthesis, (7).